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By Tag: RA

Aqueous reaction mixtures/solutions (not refluxing) under 1 M and up to 2.5 L

CEM Explorer Microwave, The use of

RA and SWP | Published | Pall Thordarson | March 20, 2012 9:31:38 AM | Keywords:Microwave reactor, RA, SWP, CEM Explorer Microwave reactor

CHRIST alpha 1-4 LDplus Freeze Dryer, operation of the (room 1001 only)

RA and SWP | Published | Pall Thordarson | October 25, 2012 1:14:19 PM | Keywords:Freeze dryer, RA, SWP, CHRIST alpha 1-4

Column chromatography (Unpressurised)

RA and SWP | Published | Pall Thordarson | September 15, 2011 11:36:53 AM | Keywords:column chromatography, gravity column chromatography, silica, alumina, columns, chemistry, RA, SWP

Decanting from drums (20 L & 200 L) - for stores only

RA and SWP | Published | Pall Thordarson | March 20, 2012 11:14:02 AM | Keywords:Decanting solvents (large scale), Solvent drums, RA, SWP, Chemical stores

Flash Column Chromatography

Hydrogenation reaction, atmospheric Pressure (only in room 232!)

RA and SWP | Published | Pall Thordarson | March 20, 2012 11:10:52 AM | Keywords:Hydrogenation, Reactions, RA, SWP, Atmospheric Pressure Hydrogenation, H2 on Pd

Medium scale (250-1000 mL) reflux reactions in air or inert atmosphere

RA and SWP | Published | Pall Thordarson | March 20, 2012 11:17:59 AM | Keywords:Reflux (< 1L), Reaction under reflux (< 1 L), Reactions in inert atmosphere, RA

NMR (routine) sample preparation and measurement

RA and SWP | Published | Pall Thordarson | March 20, 2012 11:08:28 AM | Keywords:NMR, RA, Sample preparation (NMR), Nuclear Magnetic Resonance, Proton NMR, Deuterated solvents

Pyrophoric organolithium reagents, storage, transport and use of (incl. n-BuLi, t-BuLi)

RA and SWP | Published | Pall Thordarson | March 20, 2012 11:24:21 AM | Keywords:Pyrophoric reagents, organolithium compounds, nBuLi, tBuLi, RA, SWP, reactions in inert athomsphere

Reaction mixtures/solutions (without heat) on a small scale (< 250 mL)

Rotary Evaporators

RA and SWP | Published | Pall Thordarson | September 15, 2011 11:41:36 AM | Keywords:rotary evaporator, solvent removal, chemistry, SWP, RA

Separation funnel – Liquid/Liquid extraction (< 1 L)

RA and SWP | Published | Pall Thordarson | March 20, 2012 9:44:13 AM | Keywords:Separation funnel, RA, Liquid-liquid extraction, Extractions

Small scale (< 250 mL) reflux reactions in air or inert atmosphere

RA and SWP | Published | Pall Thordarson | March 20, 2012 11:19:01 AM | Keywords:Reflux (< 250 mL), Reaction under reflux (< 250 mL), Reactions in inert atmosphere, RA

Thin layer Chromatography (TLC)

RA and SWP | Published | Pall Thordarson | September 15, 2011 11:39:58 AM | Keywords:thin column chromatography, TLC, silica, alumina, silica plates, alumina plates, chemistry, RA, SWP

UV-Vis and Fluorescence spectroscopy measurements

Vacuum pumps

RA and SWP | Published | Pall Thordarson | March 20, 2012 9:46:25 AM | Keywords:Vacuum pumps, RA, SWP, Oil pumps, Vane pumps, Diaphragm pumps, Pumps (vacuum)
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