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Pall Thordarson
Page
1
By Author: Pall Thordarson
Pyrophoric organolithium reagents, storage, transport and use of (incl. n-BuLi, t-BuLi)
RA and SWP
|
Published
|
Pall Thordarson
|
March 20, 2012 11:24:21 AM
|
Keywords
:
Pyrophoric reagents
,
organolithium compounds
,
nBuLi
,
tBuLi
,
RA
,
SWP
,
reactions in inert athomsphere
Reaction mixtures/solutions (without heat) on a small scale (< 250 mL)
RA and SWP
|
Published
|
Pall Thordarson
|
March 20, 2012 11:20:36 AM
|
Keywords
:
Reactions without heat < 250 mL)
,
Reactions
,
stirring (no heat < 250 mL)
,
Reactions in inert atmosphere
,
RA
Small scale (< 250 mL) reflux reactions in air or inert atmosphere
RA and SWP
|
Published
|
Pall Thordarson
|
March 20, 2012 11:19:01 AM
|
Keywords
:
Reflux (< 250 mL)
,
Reaction under reflux (< 250 mL)
,
Reactions in inert atmosphere
,
RA
Medium scale (250-1000 mL) reflux reactions in air or inert atmosphere
RA and SWP
|
Published
|
Pall Thordarson
|
March 20, 2012 11:17:59 AM
|
Keywords
:
Reflux (< 1L)
,
Reaction under reflux (< 1 L)
,
Reactions in inert atmosphere
,
RA
Aqueous reaction mixtures/solutions (not refluxing) under 1 M and up to 2.5 L
RA and SWP
|
Published
|
Pall Thordarson
|
March 20, 2012 11:16:11 AM
|
Keywords
:
Aqueous reaction mixtures (< 1M and < 2.5 L)
,
Aqueous solutions (< 1M and < 2.5 L
,
Aqueous solutions
,
Reactions in water
,
Water (reactions)
,
RA
,
Making aqueous stock solutions
Decanting from drums (20 L & 200 L) - for stores only
RA and SWP
|
Published
|
Pall Thordarson
|
March 20, 2012 11:14:02 AM
|
Keywords
:
Decanting solvents (large scale)
,
Solvent drums
,
RA
,
SWP
,
Chemical stores
UV-Vis and Fluorescence spectroscopy measurements
RA and SWP
|
Published
|
Pall Thordarson
|
March 20, 2012 11:12:52 AM
|
Keywords
:
UV-Vis
,
Fluorescence
,
RA
,
Spectroscopy (UV-Vis and Fluorscence)
,
Sample preparation
,
Cary 50
,
Cary Eclipse
,
Perkin Elmer
,
Cary UV-Vis
Hydrogenation reaction, atmospheric Pressure (only in room 232!)
RA and SWP
|
Published
|
Pall Thordarson
|
March 20, 2012 11:10:52 AM
|
Keywords
:
Hydrogenation
,
Reactions
,
RA
,
SWP
,
Atmospheric Pressure Hydrogenation
,
H2 on Pd
NMR (routine) sample preparation and measurement
RA and SWP
|
Published
|
Pall Thordarson
|
March 20, 2012 11:08:28 AM
|
Keywords
:
NMR
,
RA
,
Sample preparation (NMR)
,
Nuclear Magnetic Resonance
,
Proton NMR
,
Deuterated solvents
Vacuum pumps
RA and SWP
|
Published
|
Pall Thordarson
|
March 20, 2012 9:46:25 AM
|
Keywords
:
Vacuum pumps
,
RA
,
SWP
,
Oil pumps
,
Vane pumps
,
Diaphragm pumps
,
Pumps (vacuum)
Separation funnel – Liquid/Liquid extraction (< 1 L)
RA and SWP
|
Published
|
Pall Thordarson
|
March 20, 2012 9:44:13 AM
|
Keywords
:
Separation funnel
,
RA
,
Liquid-liquid extraction
,
Extractions
CHRIST alpha 1-4 LDplus Freeze Dryer, operation of the (room 1001 only)
RA and SWP
|
Published
|
Pall Thordarson
|
October 25, 2012 1:14:19 PM
|
Keywords
:
Freeze dryer
,
RA
,
SWP
,
CHRIST alpha 1-4
CEM Explorer Microwave, The use of
RA and SWP
|
Published
|
Pall Thordarson
|
March 20, 2012 9:31:38 AM
|
Keywords
:
Microwave reactor
,
RA
,
SWP
,
CEM Explorer Microwave reactor
Rotary Evaporators
RA and SWP
|
Published
|
Pall Thordarson
|
September 15, 2011 11:41:36 AM
|
Keywords
:
rotary evaporator
,
solvent removal
,
chemistry
,
SWP
,
RA
Thin layer Chromatography (TLC)
RA and SWP
|
Published
|
Pall Thordarson
|
September 15, 2011 11:39:58 AM
|
Keywords
:
thin column chromatography
,
TLC
,
silica
,
alumina
,
silica plates
,
alumina plates
,
chemistry
,
RA
,
SWP
Flash Column Chromatography
RA and SWP
|
Published
|
Pall Thordarson
|
September 15, 2011 11:38:23 AM
|
Keywords
:
flash column chromatography
,
pressurised column chromatography
,
silica
,
alumina
,
columns
,
column chromatography
,
chemistry
,
RA
,
SWP
Column chromatography (Unpressurised)
RA and SWP
|
Published
|
Pall Thordarson
|
September 15, 2011 11:36:53 AM
|
Keywords
:
column chromatography
,
gravity column chromatography
,
silica
,
alumina
,
columns
,
chemistry
,
RA
,
SWP
Page
1
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